ArabicGermanFrenchSpanishItalianPortugueseTurkishPolishRussian
International Equipments
Home / Rubber Testing Equipments / Oxidation Induction Test Apparatus (OIT / DTA)
Oxidation Induction Time — DTA / DSC Principle

Oxidation Induction Test Apparatus (OIT / DTA)

An OIT apparatus based on the Differential Thermal Analysis (DTA) principle, checking the oxidation induction time of polymers — a very sensitive test needing only 8–10 mg of sample, at 200 °C under an 80 cc/min oxygen flow.

  • Digital PID controller — up to 300 °C, resolution 0.1 °C, accuracy ±0.5 °C
  • N₂ & O₂ regulators and rotameters for stable gas flow
  • 500 SS316 aluminium pans with 40-mesh screen supplied
  • PC printout: Delta Temperature vs Time graph + OIT result
Made in IndiaISO 9001:2015CE CertifiedExported to 60+ countries
Overview

How long will the polymer resist oxidation?

Polyolefins are protected from thermal-oxidative degradation by antioxidants, and Oxidation Induction Time measures how much protection remains. A small sample (8–10 mg) is held isothermally in a reference/specimen pan pair; nitrogen is switched to oxygen and the time to the exothermic onset of oxidation is recorded. A short OIT means the stabiliser package is inadequate or depleted.

International Equipments builds an OIT apparatus on the DTA principle — barrel water-cooled, a digital PID controller to 300 °C ±0.5 °C, precision N₂/O₂ regulators and rotameters, and Indium-melting-point temperature calibration per DOT specification. Results (Delta Temperature vs Time and OIT) are graphed and printed through a PC. Manufactured in Mumbai, CE marked and calibration-certified.

How the test works

Step by step

  1. CalibrateVerify temperature calibration with Indium (m.p. 156.6 °C) under N₂.
  2. Load pansWeigh 8–10 mg of polymer into an SS316 aluminium pan with a 40-mesh screen; place the reference pan alongside.
  3. Purge & heatPurge with nitrogen and heat isothermally to the set temperature (typically 200 °C).
  4. Switch to O₂Introduce oxygen at the set flow (typically 80 cc/min) and record time to the exothermic onset.
  5. Report OITThe PC prints Delta Temperature vs Time graph with OIT result and full test metadata.
Technical Specifications

Oxidation Induction Test Apparatus (OIT / DTA) specifications

Representative specifications; configuration on request.

PrincipleDifferential Thermal Analysis (DTA)
Temperature controllerDigital PID, up to 300 °C, resolution 0.1 °C, accuracy ±0.5 °C
CoolingWater cooling of the barrel
Sample pans500 nos. SS316 aluminium pans with 40-mesh screen (per DOT spec)
Gas flow controlRegulators & rotameters for N₂ and O₂
CalibrationIndium (m.p. 156.6 °C) per DOT spec
PC printoutDelta Temperature vs Time graph + OIT result, with client, batch, operator, sample weight, gas flow, times
PaintPowder coated
Power230 V, 50 Hz, single phase
Applications

Where it's used

PE pipesDurability qualification of pressure pipe.
CablesSheathing compound stability.
GeomembranesLong-term stability of liners.
Antioxidant QCStabiliser package verification.
CertificationISO / BIS type-testing support.
R&DAntioxidant and stabiliser development.
FAQ

Frequently asked questions

What is Oxidation Induction Time (OIT)?
It is the time a polymer resists oxidation at a set temperature once oxygen is introduced — a direct measure of how effective its antioxidant package is.
Is this a DTA or DSC method?
This apparatus uses the Differential Thermal Analysis (DTA) principle; DTA and DSC methods give similar OIT results, both using a reference and specimen pan pair inside a thermal-equilibrium zone.
Why calibrate with Indium?
Indium has a fixed melting point of 156.6 °C, making it the standard reference for temperature calibration of thermal-analysis instruments under inert atmosphere.
How much sample is needed?
Only 8–10 mg — OIT is very sensitive to sample size, so a small, precisely weighed sample is used.
Get Started

Ready to specify your Oxidation Induction Test Apparatus (OIT / DTA)?

Send your material, test standard and throughput. We'll respond within one business day with a configuration and quote.

Request a Quote